C. Nickl

University of Tübingen

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Lars Wesemann

University of Tübingen

K. Eichele

Klaus Eichele

University of Tübingen

Dominik Joosten

University of Tübingen

Ulli Englert

RWTH Aachen University

A. Wagenpfeil

University of Tübingen

Mark A. Fox

Durham University

Falko M. Schappacher

University of Münster

Tobias Wütz

University of Tübingen

Torben Gädt

Technical University of Munich

Cooperative Institutions

University of Tübingen

Institute of Inorganic Chemistry of the Slovak Academy of Sciences

Technical University of Munich

University of Cologne

Universitäres Kinderwunschzentrum Lübeck

University Hospital Schleswig-Holstein

University of Münster

Ludwig-Maximilians-Universität München

University of Bergen

Bernstein Center for Computational Neuroscience Tübingen

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1,1,1‐Tris(distanna‐closo‐dodecaborat)stannat – ein tripodaler Zinnligand

Angewandte Chemie (2011)

C. Nickl Klaus Eichele Dominik Joosten Thorsten Langer Falko M. Schappacher

Zinnhaltiger Dreibeiner: Der erste tripodale Zinnligand wurde aus 1,2-Distanna-closo-dodecaborat und Zinn(II)-chlorid synthetisiert. Er besteht aus drei Äquivalenten Cluster und einem zentralen Zinnatom und bildet ein Gerüst aus sieben Zinnatomen. Seine Koordinationsfähigkeit wurde anhand der Reaktion mit [Cu(CH3CN)4]PF6 gezeigt. Dabei entsteht ein zweikerniger Kupferkomplex, dessen Dikupfereinheit verzerrt oktaedrisch von zwei Sn7-Liganden umgeben ist (siehe Schema). Detailed facts of importance to specialist readers are published as ”Supporting Information”. Such documents are peer-reviewed, but not copy-edited or typeset. They are made available as submitted by the authors. Please note: The publisher is not responsible for the content or functionality of any supporting information supplied by the authors. Any queries (other than missing content) should be directed to the corresponding author for the article.

Schema (genetic algorithms)

10.1002/ange.201100936

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Citations (6)

CCDC 827368: Experimental Crystal Structure Determination

The Cambridge Structural Database (2012)

C. Nickl K. Eichele Lars Wesemann

An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available from the CCDC and typically includes 3D coordinates, cell parameters, space group, experimental conditions and quality measures.

10.5517/ccwry9v

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CCDC 818332: Experimental Crystal Structure Determination

The Cambridge Structural Database (2011)

A. Wagenpfeil C. Nickl H. Schubert K. Eichele Mark A. Fox

10.5517/ccwgjtn

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Oxidation of germa- and stanna-closo-dodecaborate

Dalton Transactions (2015)

Torben Gädt J.-A. Dimmer S. Fleischhauer Anita Frank C. Nickl

Oxidation of group 14 heteroborates [GeB₁₁H₁₁]²⁻ and [SnB₁₁H₁₁]²⁻ yields a symmetrical dimer exhibiting a Ge–Ge bond or an unsymmetrical dimer bearing an Sn–B bond.

10.1039/c5dt00099h

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Citations (5)

1,1,1‐Tris(distanna‐closo‐dodecaborate)stannate: A Tripodal Tin Ligand

Angewandte Chemie International Edition (2011)

C. Nickl Klaus Eichele Dominik Joosten Thorsten Langer Falko M. Schappacher

Tin tripod: Starting from 1,2-distanna-closo-dodecaborate and tin(II) chloride, the first tripodal tin ligand was prepared. It is made up of three clusters and one central tin atom that build a frame of seven tin atoms. The coordination ability is illustrated by reaction with [Cu(CH3CN)4]PF6: a binuclear copper complex is formed surrounded by two Sn7 ligands (see picture).

Stannate

Tripod (photography)

10.1002/anie.201100936

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Citations (13)

CCDC 818329: Experimental Crystal Structure Determination

The Cambridge Structural Database (2011)

A. Wagenpfeil C. Nickl H. Schubert K. Eichele Mark A. Fox

10.5517/ccwgjqk

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1,2-Distanna-closo-dodecaborate—a rare example of a 1,2-distannylene ligand in transition metal chemistry

Dalton Transactions (2011)

C. Nickl Klaus Eichele Lars Wesemann

The coordination chemistry of the novel bidentate tin ligand 1,2-distanna-closo-dodecaborate is illustrated for the first time by reactions with molybdenum, platinum and gold metal complexes. Up to three clusters coordinate two metal centers in close proximity. For all these metal complexes the typical μ-bridging coordination mode was observed exclusively. Furthermore, two cluster anions react with dichloromethane via substitution of the chloride ions. The carbon functionalized tin cluster [Et(4)N](2)[CH(2)(Sn(2)B(10)H(10))(2)] and the coordination complexes [Et(3)NMe](6)[Mo(2)(CO)(6)(Sn(2)B(10)H(10))(3)], [Et(3)NMe](2)[{HPt(PEt(3))(2)(Sn(2)B(10)H(10))}(2)], [Et(4)N](2)[{HPt(PPh(3))(2)(Sn(2)B(10)H(10))}(2)] and [{(TP)Au}(2)(Sn(2)B(10)H(10))] (TP = PhP(o-Ph(2)PC(6)H(4))(2)) are fully characterized by multinuclear NMR spectroscopy, elemental analyses and crystal structure analyses.

Coordination complex

Coordination number

Cluster chemistry

10.1039/c1dt11247c

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Citations (13)

CCDC 736392: Experimental Crystal Structure Determination

The Cambridge Structural Database (2010)

C. Nickl Dominik Joosten Klaus Eichele C. Maichle-Mössmer K.W. Törnroos

10.5517/ccsq8lb

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