Mingsheng Wu

East China University of Science and Technology

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Song Cao

East China University of Science and Technology

Xuxue Zhang

Qilu Normal University

Yisen Liu

Guangdong Institute of Intelligent Manufacturing

Xianghu Zhao

East China University of Science and Technology

Xinfei Ji

Nanchang University

Juan Zhang

University of Jinan

Zhang Juan

Jialu Li

China Southern Power Grid (China)

Cao Song

Xi'an Jiaotong University

Cooperative Institutions

East China University of Science and Technology

Shanghai Institute of Technology

Shanghai Institute of Organic Chemistry

Chinese Academy of Sciences

Nanchang University

Qilu Normal University

University of Jinan

Wuhan Institute of Technology

Shandong University

China West Normal University

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LiHMDS-Promoted Palladium or Iron-Catalyzed ipso-Defluoroborylation of Aryl Fluorides

Organic Letters (2018)

Xianghu Zhao Mingsheng Wu Yisen Liu Song Cao

A novel and efficient method for the synthesis of arylboronic acid pinacol esters via a palladium- or iron-catalyzed cross-coupling reaction of aryl fluorides with bis(pinacolato)diboron (B2pin2) in the presence of LiHMDS was developed. The Pd-catalyzed defluoroborylation of fluoroarenes is compatible with a variety of functional groups such as primary and secondary amine, ketone, trifluoromethyl, alkoxy, and boryl. Remarkably, no external ligand is required for enhanced conversion efficiency.

Pinacol

Primary (astronomy)

10.1021/acs.orglett.8b02228

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Facile Synthesis of 3-Arylindenes by HMPA-Promoted Direct Arylation of Indenes with Aryl Fluorides

ACS Omega (2018)

Xinfei Ji Jialu Li Mingsheng Wu Song Cao

A rapid and efficient approach to 3-arylated indenes by reactions of indenes with unactivated fluoroarenes with the assistance of lithium diisopropylamide and hexamethylphosphoramide at room temperature was developed.

Lithium diisopropylamide

Hexamethylphosphoramide

10.1021/acsomega.8b01542

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Synthesis of N,N-disubstituted 2-aminothiophenes by the cyclization of gem-difluoroalkenes with β-keto thioamides

Organic & Biomolecular Chemistry (2017)

Xuxue Zhang Mingsheng Wu Juan Zhang Song Cao

A novel and effective method for the construction of highly functionalized aminothiophenes via the cyclization of gem-difluoroalkenes with β-keto tertiary thioamides is described. The reactions proceed smoothly with the assistance of K2CO3 under transition-metal-free conditions, affording a variety of valuable N,N-disubstituted 2-aminothiophenes in moderate to good yields.

10.1039/c7ob00368d

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Citations (21)

Synthesis of difluoromethylated enynes by the reaction of α-(trifluoromethyl)styrenes with terminal alkynes

Organic & Biomolecular Chemistry (2018)

Mingsheng Wu Xianghu Zhao Yisen Liu Song Cao

A novel and efficient method for the synthesis of difluoromethylated enynes by the reaction of α-(trifluoromethyl)styrenes with terminal alkynes with the assistance of NaOtBu was developed.

10.1039/c8ob02117a

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Citations (6)

gem‐ジフルオロアルケンとβ‐ケトチオアミドの環化によるN,N‐二置換2‐アミノチオフェンの合成

Organic & Biomolecular Chemistry (2017)

Xuxue Zhang Mingsheng Wu Zhang Juan Cao Song

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